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MGBR

Triflidic acid

following route: (1) Tf2CH2 + 2 CH3MgBr → Tf2C(MgBr)2 + 2 CH4 (2) Tf2C(MgBr)2 + TfF → Tf3C(MgBr) + MgBrF (3) Tf3C(MgBr) + H2SO4 → Tf3CH + MgBrHSO4 In its anionic

Diethylphosphite

CH3MgBr → (C2H5O)2P(O)MgBr + CH4 (C2H5O)2P(O)MgBr + 2 CH3MgBr → (CH3)2P(O)MgBr + 2 MgBr(OC2H5) (CH3)2P(O)MgBr + H2O → (CH3)2P(O)H + MgBr(OH) Diethyl phosphite

Diphenylphosphine oxide

followed by acid workup: (C2H5O)2P(O)H + 3 C6H5MgBr → (C6H5)2P(O)MgBr + C2H5OMgBr (C6H5)2P(O)MgBr + HCl → (C6H5)2P(O)H + MgBrCl Alternatively, it may be prepared

Phenylsilane

Ph−Si(OEt)3 product with LiAlH4 affords phenylsilane. Ph−MgBr + Si(OEt)4 → Ph−Si(OEt)3 + MgBr(OEt) 4 Ph−Si(OEt)3 + 3 LiAlH4 → 4 Ph−SiH3 + 3 LiAl(OEt)4

Dimethylphosphine oxide

equations: (C2H5O)2P(O)H + 3 CH3MgBr → (CH3)2P(O)MgBr + 2 MgBr(OC2H5) + CH4 (CH3)2P(O)MgBr + H2O → (CH3)2P(O)H + 2 MgBr(OH) Chlorination gives dimethylphosphoryl

Triethyl orthoformate

Bodroux–Chichibabin aldehyde synthesis, for example: RMgBr + HC(OC2H5)3 → RC(H)(OC2H5)2 + MgBr(OC2H5) RC(H)(OC2H5)2 + H2O → RCHO + 2 C2H5OH In coordination chemistry, it

Carbon dioxide

compounds react with CO2 to give carboxylates: MR + CO2 → RCO2M where M = Li or MgBr and R = alkyl or aryl. In metal carbon dioxide complexes, CO2 serves as a

Alkylation

(Ar-Br) reacts with nickel with ligands (NiL2). Then, a Grignard reagent (R-MgBr) alkylates the nickel center, replacing the bromide ligand (Br) with an alkyl

Coupling reaction

Reaction Year Reactant A Reactant B Catalyst Remark Grignard reaction 1900 R-MgBr sp, sp2, sp3 R-HC=O or R(C=O)R2 sp2 not catalytic Gomberg–Bachmann reaction

Phenethyl alcohol

C6H5MgBr + (CH2CH2)O → C6H5CH2CH2OMgBr C6H5CH2CH2OMgBr + H+ → C6H5CH2CH2OH + MgBr+ Phenethyl alcohol can also be produced by biotransformation from L-phenylalanine